Thermal-analysis

Differential Scanning Calorimetry(DSC) Analysis and testing service

Shanghai Jituo Hi-tech provide DSC testing services. Differential scanning calorimeter can be used for the determination of specific heat capacity, crystallinity, glass transition temperature and melting point.

Differential Scanning Calorimetry (DSC)

DSC is a thermal analysis technique developed from Differential Thermal Analysis (DTA). It is defined as a method for measuring the heat flow of a sample relative to a reference material under temperature program control, abbreviated as DSC (Differential Scanning Calorimetry). DSC technology facilitates quantitative data acquisition for thermal effects while retaining DTA functions. It is widely used to: Determine melting heat, crystallinity, and isothermal crystallization kinetic parameters of polymers;

  • Measure glass transition temperature (Tg);
  • Study reactions such as polymerization, curing, crosslinking, and decomposition;
  • Determine reaction temperature/zone, reaction heat, and kinetic parameters.

Instrument Performance and Technical Parameters

  • Model: TA Q2000
  • Temperature Range: -75°C to 550°C (wide temperature coverage for multi-scenario thermal analysis)
  • Temperature Accuracy: ±0.01°C (high-precision temperature control, data repeatability ≤±0.5%)
  • Heating Rate: 0.1–100°C/min (supports conventional scanning and ultrafast kinetic research)
  • Atmosphere Control: Nitrogen (N₂, 50 mL/min standard), customizable oxidizing atmosphere (advance application required)

Sample Requirements and Preparation Specifications

  • Sample State Solid (powder/particles/film), liquid, gel
  • Sample Amount 5–20 mg , <1 mg (micro-quantity)
  • Drying Requirement Complete removal of solvents/moisture

DSC Testing cases

DSC测试结晶与熔融.jpg DSC测试玻璃化温度.jpg DSC 反应动力学研究.jpg DSC比热容测试.jpg

Reference Standards and Hyphenated Technologies

Testing ItemInternational/Industry StandardsHyphenated Technology Expansion
Glass Transition TemperatureASTM E1356, ISO 11357-2*DSC-TGA Hyphenation (ASTM E1131)
Melting/Crystallization Behavior AnalysisASTM D3418, ISO 11357-3*EGA-IR Hyphenation (ISO 11358)
Oxidative Induction Time (OIT)ASTM D3895, ISO 11357-6*-
Specific Heat Capacity MeasurementASTM E1269, ISO 11357-4*-