Pyrolysis chromatography is an effective analytical technique that decomposes non-volatile molecules into fragments suitable for chromatographic analysis by heating, thus generating a reproducible characteristic fingerprint of non-volatile samples. This technique can be applied in many different fields.
Instrument Model and Parameters
- Instrument Model: GCMS-QP2010Ultra, EGA/PY-3030D
- Technical Parameters:
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- Mass range: 15–2000 amu
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- Resolution: m/z=0.1
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- Scanning speed: 5,200 u/second
Sample Submission Requirements and Notes
- Sample form: Solid or liquid, 20–100 mg in a plastic centrifuge tube.
- Before testing, the pyrolysis temperature and pyrolysis method of the sample must be determined (TGA testing can be conducted in advance).
Testing Cases
Reference Standards
- GB/T 39699-2020 "Identification of rubber polymers - Pyrolysis gas chromatography-mass spectrometry"
- GB/T 29613.1-2013 "Rubber - Pyrolysis gas chromatography analysis - Part 1: Identification of polymers (single and blended)"
- GB/T 39560.8-2021/IEC 62321-8-2017 "Determination of certain substances in electrical and electronic products - Part 8: Determination of phthalates in polymers by gas chromatography-mass spectrometry (GC-MS) and gas chromatography-mass spectrometry with pyrolysis/thermal desorption (Py/TD-GC-MS)"
- SN/T 4565-2016 "Determination of tris(2-chloroethyl) phosphate in polymer materials of electrical and electronic products - Pyrolysis-gas chromatography-mass spectrometry qualitative screening method"
- SN/T 5297-2021 "Determination of hexabromocyclododecane in polymer materials of electrical and electronic products - Pyrolysis-gas chromatography-mass spectrometry qualitative screening method"
