NMR_MS

Nuclear Magnetic Resonance(NMR) analysis and testing service

Shanghai Jituo Hi-tech provides NMR testing services. Nuclear magnetic resonance detection can be used for 1H NMR, 13C NMR, and other spectral tests such as 9F, 31P, 29Si, and 17O NMR.

NMR testing (Nuclear Magnetic Resonance) is used for determining the structure of organic compounds, analyzing their qualitative characteristics, and quantitatively measuring the relative content of compounds. The principle of NMR (Nuclear Magnetic Resonance) is based on the different spin behaviors of atomic nuclei, and the compound structure is inferred from the nuclear displacement. NMR is a crucial tool for structural identification of organic compounds, typically identifying functional groups by chemical shifts, determining bonding relationships through coupling splitting peaks and

Instrument Model and Parameters

  • Instrument Model: Bruker AVANCE III HD 400 MHz
  • Technical Parameters:
    • 400 MHz
    • Resolution: m/z-0.1H
    • Resolution < 0.35 Hz, S/N > 165:1 (for 13C)
    • Resolution ≤ 0.13 Hz, S/N > 1913 147:1
    • 31P: S/N > 150:1
    • 9F: S/N > 125:1

Sample Submission Requirements and Notes

  • Sample form: Solid or liquid, 20–100 mg in a plastic centrifuge tube.
  • The sample must be completely soluble in common volatile solvents (water, toluene, DMSO, methanol, chloroform, etc.).

Testing Cases

1H-NMR.jpg 13C NMR.jpg

Reference Standards